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Spectral Interpretation Workbooks
Links
WebSpectra - Problems in NMR
http://www.chem.ucla.edu/~webspectra/
More NMR practice problems and a great outline of spectral assignments methods.
Organic Structure Elucidation Workbook
http://www.nd.edu/~smithgrp/structure/workbook.html
A set of NMR stucture determination and assignment problems, easy, moderate and hard. (Select "problems" from left frame)
Proton NMR Tutorial
http://www.wfu.edu/~ylwong/chem/nmr/h1/
Tutorial and exercises on nuclear magnetic resonance.